By A. G. Sykes, Alan H. Cowley
Advances in Inorganic Chemistry provides well timed and informative summaries of the present growth in various topic parts inside inorganic chemistry, starting from bioinorganic to reliable nation. This acclaimed serial gains reports written by means of specialists within the quarter and is an integral connection with complex researchers. every one quantity of Advances in Inorganic Chemistry comprises an index, and every bankruptcy is absolutely referenced. learn more... summary: Advances in Inorganic Chemistry offers well timed and informative summaries of the present growth in various topic components inside inorganic chemistry, starting from bioinorganic to sturdy country. This acclaimed serial beneficial properties reports written via specialists within the quarter and is an critical connection with complicated researchers. every one quantity of Advances in Inorganic Chemistry comprises an index, and every bankruptcy is absolutely referenced
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9 Hz) below Ϫ20ЊC. Several diphosphino–phosphide complexes of lithium have also been reported (64). Reaction of R2P-P(SiMe3)-PRЈ2 with BunLi yields the monomeric complexes [(L)Li͕R2P-PPRЈ2͖] [R ϭ RЈ ϭ But, L ϭ (THF)2 , tmeda; R ϭ But, RЈ ϭ Pri, L ϭ (THF)2 ; R ϭ RЈ ϭ Pri, L ϭ (THF)2 ; R ϭ But , RЈ ϭ NEt2 , L ϭ (THF)2 ], which have all been crystallographically characterized. In each case the diphosphino–phosphide ligands bind through the two R2P groups, there is no contact between the phosphido center and lithium; the lithium atoms achieve a distorted tetrahedral geometry by coordination to the donor atoms of the coligand(s).
81 A) but longer than the typical car˚ (51). 61 A demonstrated that imidazol-2-ylidenes will also react with selenium or tellurium to produce the selenones 77 and tellurones 78 (54, 55). It is of interest to note that in general tellurocarbonyl compounds, such as telluroaldehydes, can only be isolated by stabilization with metals (56), whereas 78 is relatively stable (57). The crystal structures of 77 and 78, in concert with 125Te and 77Se NMR data, respectively, support an ylidic structure in both cases, rather than a formal double bond.
Cowley, A. ; Dias, H. V. ; Goerlich, J. ; Marshall, W. ; Riegel, B. Inorg. Chem. 1997, 36, 2151. 45. Arduengo, A. , III; Dias, H. V. ; Calabrese, J. C. Chem. Lett. 1997, 143. 46. Arduengo, A. , III; Carmalt, C. ; Clyburne, J. A. ; Cowley, A. ; Pyati, R. Chem. Commun. 1997, 981. 47. ; Waskowska, A. Chem. Ber. 1981, 114, 3289. 48. ; Burg, A. B. J. Am. Chem. Soc. 1958, 80, 6161. 49. ; Bunghardt, D. Z. Anorg. Allg. Chem. 1987, 549, 73. 50. Arduengo, A. ; Marshall, W. ; Schmutzler, R. J. Am. Chem.
Main Group Chemistry by A. G. Sykes, Alan H. Cowley